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Beilstein J. Org. Chem. 2016, 12, 1987–2004, doi:10.3762/bjoc.12.186
Graphical Abstract
Scheme 1: PTSA-catalyzed diazotization and azo coupling reaction.
Scheme 2: Ferric hydrogen sulfate (FHS) catalyzed azo compound synthesis.
Scheme 3: Synthesis of azo compounds in the presence of silica supported boron trifluoride.
Scheme 4: Phase transfer catalyzed azo coupling of 5-methylresorcinol in microreactors.
Scheme 5: Synthesis of yellow pigment 12 in a micro-mixer apparatus.
Scheme 6: Continuous flow synthesis of Sudan II azo dye in LTF-MS microreactors.
Figure 1: pH profile plot at constant flow rate of 0.03 mL/min.
Figure 2: pH profile plot at a constant flow rate of 0.7 mL/min.
Scheme 7: Azo coupling reaction under acidic conditions.
Figure 3: pH profile plot at a constant flow rate of 0.03 mL/min.
Figure 4: pH profile plot at constant flow rate of 0.7 mL/min.
Figure 5: Temperature profile plot at constant pH 5.66.
Figure 6: Schematic representation of the microreactor set up.
Figure 7: Schematic representation of the microreactor set up.
Figure 8: Scaled up microreactor set up: PTFE tubing i.d. 1.5 mm a) Chemyx Fusion 100 classic syringe pump, b...